manufacturer:       Transgenomic

model:                   WAVE

annotation:           Dokumente engl.

Hitachi D-7000/D-6000 Interface Module

Product Specifications

Enclosure

The D-7000 IFM enclosure has the following physical characteristics:

• Dimensions                 260 mm x 500 mm x 50 mm (W x L x H)
• Weight                                     6 kg
• Power Supply             25 VA

CPU Board

• CPU                             68340 (16 MHz)
• ROM                            256K
• RAM                             1.0 MB
• I/O RAM                       256K

A/D Converter

• Analog Range             -10 mV to 1 V
• Dynamic Range          21 bits
• Resolution                   0.25 microvolts per count
• Minimum A/D Speed 12.5 msec.

Hitachi L-7100 Pump

Specifications

Pump Unit

(1)                Liquid feed system: Dual plunger type reciprocating pump, series connection

(2)                Maximum discharge pressure: 39.2 MPa (400 kgf/cm²)

(3)                Discharge rate range: 0.001 to 9.999 mL/min

(4)                Pressure limit range: 0 to 41.2 MPa

(5)                Discharge volume of plunger no. 1: 100 µL/stroke

(6)                Flow rate setting accuracy (at constant room temperature of 20°C for distilled water):

• ±2 µL/min (0.01 to 0.1 mL/min, 1.0 to 39.2 MPa)
• ±2% (0.101 to 5 mL/min, 1.0 to 39.2 MPa)
• ±2% (5.001 to 9.999 mL/min, 1.0 to 2.0 MPa)
• +2% to -1p*% of discharge pressure

(5.001 to 9.999 mL/min, 2.1 to 39.2 MPa)

*p          Pump pressure (MPa)

(7)    Flow rate stability: 0.2% RSD or less (retention time at flow rate 1 mL/min, at constant room temperature of 20°C for distilled water)

(8)                Compensation of solvent compression ratio and elimination of pulsation:

High-speed feedback real-time control

(9)                Pressure display accuracy: ±5%

(10)            Constant pressure liquid feed:

2.0 to 39.2 MPa (20 to 400 kgf/cm²) (Flow rate range: 0 to 5 mL/min)

(11)            Material of wetted parts:

SUS 316, ruby, sapphire, ceramic, PTFE carbon-impregnated PTFE

(12)            Display data:

Parameters

Pump monitor            Flow rate, pressure

Gradient monitor         Elapsed time, mixing ratio, flow rate,

pressure, timer value, etc.

(13)            Pump control mode:

• Single-liquid delivery mode
• Low pressure gradient mode
• High pressure gradient mode

(14)            Contact input/output terminals:

Event timer: 4 channels

(15)            External communication:

D-line

(a) D-line communication mode ( D-line ON )

(b) D-line contact mode (D-line OFF)

OUTPUT PUSY/READY

INPUT             1) GRADIENT START

2) EMERGENCY STOP

(16)            Specification of pressure unit: MPa, kgf/cm², bar, psi

(17)            Pressure zero adjustment:

Possible

(18)            Ambient temperature:

4 to 35°C (condensation unallowable)

(19)            Humidity:

45 to 85% RH

(20)            Power supply:

100 to 240 V AC ± 10%

(21)            Power frequency:

50/60 Hz

(22)            Power consumption:

About 100 VA

(23)            Dimensions:

260 (W) x 500 (D) x 150 (H) mm

(24)            Weight:

About 14 kg

(25)            Installation Category:

II (by IEC1010-1 Annex J)

Low Pressure Gradient System

(1)                Number of mobile phase

UP to 4

(2)                Mixing  

Valve opening/closing time control

(3)                Mixing ratio range

0 to 100% (in increments of 1%)

(4)                Flow rate setting range

0.001 to 9.999 mL/min (in increments of 0.001 mL/min)

(5)                Recommended flow rate range

0.1 to 9.999 mL/min

(If the flow rate exceeds 2.0 mL/min, it is recommended to use the optional mixer.)

(6)                Gradient elution profile

Linear/multi-step

(7)                Number of programming steps

92 steps max. per program

100 steps max./9 programs

(8)                Programming time

Up to 600 min (in increments of 0.1 min)

(9)                Programming items

§          B/C/D mixing ratio

§          Flow rate

§          Event Signal output

§          Pump stop, buzzer

(10)            Number of programs

9

High Pressure Gradient System

(1)                Number of mobile phase

Up to 3

(2)                Mixing

Double or triple pump flow rate control

(3)                Mixing ratio range

0.0 to 100.0% (in increments   of 0.1%)

(4)                Flow rate setting range

0.001 to 9.999 mL/min (in increments of 0.001 mL/min)

(5)                Recommended flow rate range

0.1 to 9.999 mL/min

(6)                Gradient elution profile

Linear/multi-step

(7)                Number of programming steps

92 steps max. per program

100 steps max./9 programs

(8)                Programming time

Up to 600 min (in increments of 0.1 min)

(9)                Programming items

§          B/C mixing ratio

§          Flow rate

§          Event Signal output

§          Pump stop, buzzer

(10)            Number of programs

9

Dynamic Mixer (Option)

Outline

This mixer is used to enhance the mixing accuracy of two or more mobile phases through forcible stirring and thereby stabilize the baseline.

It is combined with a high pressure gradient system or low pressure gradient system. Refer to section 3-7-2 for usage of the low pressure gradient system.

Specifications of Dynamic Mixer

(1)                Stirring method

With stirrer

(2)                Chamber capacity

About 2.0 mL (0.69 mL x 1, 0.65 mL x 2)

(3)                Rotational speed

300 rpm (fixed)

(4)                Withstand pressure

34 MPa (350 kg/cm²)

(5)                Maximum working flow

9.999 mL/min

(6)                Recommended working flow range

0.1 to 9.999 mL/min

(7)                Rating

12 V DC, 0.5 A

(8)                Dimensions

65(W) x 42(D) x 93(H) mm

Merck Solvent Degasser L-7612

Conforms to EC Low Voltage Standard 73/23/EC

Technical Data

(1)                Voltage

220 Volt/50 Hz

(2)                Tolerable voltage range

±10%

(3)                Power consumption

50 watts

(4)                Material in contact with liquid

Teflon, PEEK and tefzel (fitting/ferrule)

(5)                Degassing channels

4

(6)                Optimal flow

0.1 - 3.0 ml/min. per channel

(7)                Dead volume per channel

8 ml (+/- 10%)

(8)                Membrane surface area

approx. 250 cm²

(9)                Liquid connections

1/4-28"

(10)            Weight

3.8 kg

(11)            Dimensions

160 (h) x 80 (w) x 320 (d) mm