Perkin Elmer 200
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Objektnummer | B00011594 |
---|---|
ID-Nummer | 011594 |
Objektbezeichnung | Perkin Elmer 200 |
Status | Archiv |
Status, Liefer- und Zahlungsbedingungen
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Firma: Perkin Elmer
The following illustrations and descriptions are referring to the instrument model and are drawn from brochures. They are not representating the delivery volume. The exact delivery content you will find only in the offering text.
Series 200 LC-Pump
The series 200 LC Pump
The Perkin-Elmer Series 200 LC Pump can be used with virtually every LC system or application. The Series 200 LC Pump is upgradable from a single solvent (isocratic) pump, to mixing two solvents (binary) or to mixing four solvents (quaternary). In addition, each version is available in a biocompatable version. The Series 200 LC Pump provides you with the interchangeable technology so that you do not have to buy a new pump and learn new user interfaces every time your needs change.
Series 200 LC Pump Features and Benefits
Upgradable isocratic, binary, and quaternary versions as well as biocompatible versions for maximum flexibility.
Small, compact design (12 inches (30.5 cm) wide) saves valuable bench space.
Directory of up to 20 methods, 20 steps each with built-in method linking increases sample throughput.
Edit the active method or sequence in real-time with easy access function keys.
Large backlit liquid crystal display allows clear viewing of pump method and operating parameters at all times.
Unique function allows automatic shutdown of the pump method at final gradient method.
Graphic display of solvent profile on-screen shows real-time status of the gradient method.
Hold gradients or advance to the next step with a simple keystroke.
Solvent-resistant front panel with rounded ergonomic design for easier interaction with the keypad.
Tactile keyboard with unique "key click" so that you know your entry has been made.
Phone-type contact closure connections and finger tight plumbing Fittings make it simple to connect or disconnect your system.
Full method documentation including modification with method name, number, date and time stamp.
Visual access front-door panel allows quick plumbing inspection and easy servicing.
Maintenance log coded by the serial number of the pump, including pump and seal cycles.
Instrument log records history of operation for quick diagnosis and servicing to get you up and running quickly.
Extensive service diagnostics.
Pump module can be completely removed to lab bench for maintenance without having to unstack modules.
Specification
General Specifications
Flow Rate Range |
0.01 to 10.0 mL/min (maximum pressure of 6 200 psi (420 bar) over the entire range |
Flow Rate Increments |
0.01 from 0 to 0.99 mL/min and 0.1 from 1.0 to 10.0 mL/min |
Flow Precision |
0.3% relative standard deviation (typically <0.1%) at 1 mL/min and 1 000 psi (70) bar with water as the mobile phase |
Flow Accuracy |
±1% of the setting at 1 mL/min and 1 000 psi (70 bar) with water as the mobile phase |
Retention Time Reproducibility |
<0.3% RSD (typically <0.1% RSD) |
Pressure Range |
0 to 6 200 psi or 0 to 420 bar from the entire flow-rate range |
Pressure Limits |
High and low limit user-settable to 10 psi or 1 bar increments |
Solvent Compressibility |
Keyboard settable flow calibration |
Composition Range |
0 to 100% solvent A - D (depending on your pump configuration) |
Composition Settability |
Settable to 0.1% |
Composition Accuracy |
±1.0% absolute from 3 to 97% at 5 mL/min |
Composition Precision |
Typically less than 0.2% variation |
Gradient Curves |
Linear, exponential 1 to 9.9 (positive and negative), or step (89 profile selections) |
Linearity |
Within ±1% from 10 to 90% at 5 mL/min |
Program Steps |
Step 0 plus up to 20 solvent program steps. Battery-backed storage of up to 20 methods plus one default method. |
Step Time |
0 to 999 min |
Step Time Increments |
0.1 min, 0 to 9.9 min; 1.0 min, 10 to 99 min |
Programmed Timed Events |
Two built-in independent momentary (two second) contact closures |
Events/Methods |
Maximum of 20 |
Event Increments |
0.1 min, 0 to 9.9 min; 1.0 min, 10 to 99 min |
Dimensions (HxWxD) |
14 cm x 30.5 cm x 43 cm |
Weight |
15.9 kg (35 lbs.) |
Operating Specifications
Operating Conditions: |
|
Environment |
This instrument is designed for indoor use. It is not designed to operate in an explosive environment. |
Ambient temperature |
10 - 35°C |
Ambient relative humidity |
20 - 80% (without condensation) |
Altitude |
0 to 2000 meters |
Installation Category |
This instrument is able to withstand transient overvoltage according to Installation Category II as defined in IEC 1010-1. |
Pollution Degree |
This instrument will operate safely in environments that contain nonconductive foreign matter to Pollution Degree 2 in IEC 1010-1. |
Storage Conditions: |
|
Ambient temperature |
-20 to 60°C (-4 to 140°F) |
Ambient relative humidity |
20 - 80% (without condensation) |
Altitude |
0 to 12,000 meters |
Electrical Specifications
AC Power Requirements: |
|
AC power |
70 Watts |
AC voltage range |
Grounded 100, 120, 220, 230, VAC (±10%) Grounded 240 VAC (+6%/-10%) |
Frequency |
50/60 Hz (±1%) |
Fuse rating characteristics: |
|
100/120 VAC Single Fuse |
1.6 A 3 AG Slow Blow, 250 V |
220-240 VAC Single/Dual Fuse |
0.8 A TT (5x20 mm), 250 V |
Series 200 Autosampler
Figure 1-1. The Series 200 LC Autosampler.
The Perkin-Elmer Series 200 LC Autosampler is an advanced sample processor that can be used with virtually every liquid chromatography system or application. You configure the Autosampler and define all of your methods and operations using function keys on a keyboard located on the front panel of the instrument. A backlit Liquid Crystal Display (LCD) located directly above the keyboard shows both status information about the instrument and provides access to the screens you use to define methods and set configuration parameters. If you use the Perkin-Elmer Series 200 LC Pump, you will find that the Autosampler front panel is almost identical to the one on the Pump. In addition, the Pump and the Autosampler share many common operating features that will allow you to get your system up and running quickly. The Series 200 LC Autosampler provides you with interchangeable technology so that you do not have to buy a new Autosampler and learn new user interfaces every time your needs change.
Series 200 LC Autosampler Features and Benefits
Upgradable to biocompatible versions for maximum flexibility.
Small, compact design (12.5 inches (31.8 cm) wide) saves valuable bench space.
Directory of up to 20 methods.
Ability to link up to 10 methods together in a sequence.
Priority method which allows you to interrupt a method or sequence to run critical samples. The method or sequence resumes once the priority samples are analyzed.
Edit the active method or sequence in real-time with easy access function keys.
Large backlit liquid crystal display allows clear viewing of autosampler method and operating parameters at all times.
Tactile keyboard with unique "key click" so that you know your entry has been made.
Phone type contact closure connections and finger tight plumbing fittings make it simple to connect or disconnect your system.
Full method documentation including modification with method name, number, date and time stamp.
Visual access front-door panel allows quick plumbing inspection and easy servicing.
Maintenance log coded by the serial number of the autosampler, including autosampler injection cycles.
Instrument log records history of operation for quick diagnosis and servicing to get you up and running quickly.
Extensive service diagnostics.
Sampler module can be completely removed to lab bench for maintenance without having to unstack modules.
Specification
Injection range |
Programmable from 0.1 - 1.0 µL at 0.1 µL increments, 1 µL to 2.5mL at 1µL increments |
Replicate injections |
1 - 99 from one vial |
Precision |
Typically <0.5% RSD of peak areas from 3 µL |
Linerarity |
>0.999 |
Minimum sample volume |
1 µL in 7 µL |
Sample syringe sizes |
50, 100, 250, 500, 1000, 2500 µL |
Sample waste |
None (or user selectable) |
Carryover |
<0.02% |
Flush cycles |
User selectable, 1 - 9 |
Flush volume |
0 - 2500 µL |
Sample capacity |
up to 225 vials with optional tray |
Method parameters |
Injection volume, sample draw speed, flush volume, flush cycle, 2 external contacts, start and stop time |
Methods |
Battery-backed storage of up to 20 methods including time programming. Editing of stored methods possible during runs. |
Injection cycle time |
2 - 3 samples per minute |
Valve materials in contact with sample |
With Rheodyne 7725 for Analytical - stainless steel, Vespel, ceramic, PEEK With Rheodyne 9725 for Bio Applications - PEEK, Tefzel, ceramic With Rheodyne 8125 for Microbore - stainless steel, Vespel, ceramic, PEEK |
Display |
7-line by 40-character backlit liquid crystal display |
Communications |
Integrated communications for derivatization and dilution options Serial communications - standard BCD interface - standard 5 relay outputs; 2 timed events, 2 inject, 1 start |
AC Power Requirements: |
|
AC power |
70 Watts |
Specification
AC voltage range |
Grounded 100, 120, 220, 230, VAC (±10%) Grounded 240 VAC (+6%/-10%) |
Frequency |
50/60 Hz (±1%) |
Fuse rating characteristics: |
|
100/120 VAC Single Fuse |
1.6 A 3 AG Slow Blow, 250 V |
220-240 VAC Single/Dual Fuse |
0.8 A TT (5x20 mm), 250 V |
Operating Conditions: |
|
Environment |
This instrument is designed for indoor use. It is not designed to operate in an explosive environment. |
Ambient temperature |
10 - 30°C |
Ambient relative humidity |
10 - 80% (without condensation) |
Altitude |
0 to 2000 meters |
Installation Category |
This instrument is able to withstand transient overvoltage according to Installation Category II as defined in IEC 1010-1. |
Pollution Degree |
This instrument will operate safely in environments that contain nonconductive foreign matter to Pollution Degree 2 in IEC 1010-1. |
Peltier sample cooling tempera- ture range |
4 - 50°C, ± 2°C |
Storage Conditions: |
|
Ambient temperature |
-20 to 60°C (-4 to 140°F) |
Ambient relative humidity |
10 - 80% (without condensation) |
Altitude |
0 to 12,000 meters |
Dimensions |
Height: 400 mm (15.8 in) Width: 318 mm (12.5 in) Depth: 483 mm (19 in) |
Weight |
21 kg (461bs) |
DAD-Detector LC-235C
The LC-135C and LC-235C multiple wavelength diode array LC detectors contain the following features:
Individual signal amplification of each pixel for a significantly improved signal-to-noise ratio.
Automatically determines peak purity by an absorbance index technique, for dependable data, even on trace levels of sample.
A dual beam design using two 35-element diode arrays provides excellent baseline stability at all wavelengths and all solvent systems.
History File reports (records of detector conditions for the run) are printed at the end of each run.
Automatically annotates the wavelength of maximum absorbance on each peak.
Biocompatible solvent path.
Instantaneous wavelength change.
All wavelengths monitored at the same time.
Computerized diagnostics.
In addition, the LC-235C Diode Array Detector contains the following features:
Produces instantaneous spectra.
Plots the spectra.
Overlays the spectra.
Normalizes the spectra.
Constructs an Absorbance Profile Map.
Contains the option of selectable modes of spectral acquisition.
Produces automated background correction of spectra.
Specifications
Optical System Dual beam polychromator.
Source Deuterium lamp.
Spectral Bandwidth 5 to 175 nm.
Wavelength Range 195 to 365 nm.
Wavelength Accuracy < 1 nm.
Noise < 5 x 10 -5 AU P/P at 240 nm, and 15 nm bandwidth at peak width setting of 16 sec.
Drift < 2 x 10 -4 AU/hour at 240 nm, after warmup.
Absorbance Range -0.3 to 1.0 AU.
(on the optional plotter)
Linear Absorbance Range ≤1% deviation to 1.5 AU.
Flowcell Standard 8-µL volume, 10-mm pathlength, titanium. Dispersion: 20 µL, four sigma. Built-in holmium oxide filter.
Flowcell Pressure Rating 2200 psi
Analog Signal Outputs Two outputs, for wavelengths A and B,
(integrator) with software-selectable output voltage and filtering.
Number of Methods Nine user-programmable methods plus Method 0. Protected memory.
Nine steps per method.
Chromatograms and Spectra* Printer/plotter output.
Spectral Storage* 1000
Spectral Library* 21 in protected memory. Dimensions:
Height 28 cm (11 in.)
Width 36 cm (14 in.)
Depth 46 cm (18 in.)
Weight 25 kg (55 lb.)
Electrical Requirements 120/220 V, 50/60 Hz
Power Consumption 100 watts