HPLC systemen

Waters Alliance 2695

€ 10.486,00
Excl. 19% VAT , excl. Shipping Cost
€ 12.478,34 incl. Vat
Seriennummer: 38005
Status: Stock unit?The device is in our stock, however, has to be inspected by our technician, in order to be able to guarantee complete function.
Verzending: 10-14 werkdageniFor incoming orders until 12:00 (German local time). If customs handling is required, shipment will be delayed.
Beschrijving:
Waters HPLC Alliance 2695. Bestaande uit:
Fluorescentiedetector 2475.
DAD-detector 996.
kolom oven.
ontgasser.
230 V. 50/60 Hz.
Installation
De installatie van dit laboratoriumapparaat voeren wij vakkundig uit. Wij bieden u graag de installatie van dit laboratoriumapparaat aan voor: 1120€, exclusief reiskosten.

Usually, laboratory and analysis devices are very exigent system with a very own specifications and requirements. Therefore, the startup of a laboratory device often rises the question how to assemble, adjust and to launch it.


We would be pleased to take over the professional installation of your laboratory devices!

Please contact us.


Benefit from the installation by us in more than one way:

  • Immediate and smooth startup of your laboratory device
  • A professional installation extends the lifetime of your laboratory device
  • Guarantee extends to 3 months
  • Freight charges do not apply*
  • You are entitled to benefit from the Labexchange Repurchase Guarantee.

* products of the product groups laboratory furniture and laminar flow are excluded. In individual cases, other product groups can be excluded.


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Meer informatie
Objektnummer B00038005
Seriennummer 38005
Object Naam Waters Alliance 2695
Status Lagergerät
Fabrikant Waters
Verzending 10-14 werkdagen

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Nederland, België en Luxemburg

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Betaling via factuur is mogelijk voor ondernemingsklanten.

Andere landen

vooruitbetaling

 

 

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nieuw

Dit is een artikel dat nieuw van de fabriek komt. Hiervoor gelden de garantiebepalingen en wettelijke garantietermijn van de fabrikant.

manufacturer :       Waters

model :                   Alliance

annotation :           Dokumente engl.

 

Separations Module 2790

The Waters 2790 Separations Module integrates a solvent management system and a three-axis Sample management system to provide high-throughput analysis for HPLC, LC/MS, or flow injection-mass spectrometry applications.

 

 

Components

The 2790 Separations Module consists of:

•            Three-axis (XYZ) sample management system

•            HPLC solvent delivery system

•            Four-channel inline vacuum degasser (one channel reserved for sample management purge solvent)

•            Integral plunger seal-wash system

•            LCD display

•            Keyboard

•            Floppy dick drive (using 3.5-inch floppy disks)

•            Column heater (optional)

•            Sample heater/cooler (optional)

•            Column selection valve (optional)

•            Bar code reader (optional)

When the 2790 Separations Module with the optional sample heater/cooler is installed with the 2790 column heater, it is known as the 2790XE. Refer to Section B.3, 2790 Module Options, for Information about the 2790 Separations Module options.

 

Operating Modes

The 2790 Separations Module can operate as a stand-alone HPLC system controller, as an HPLC system controlled by Millennium@ 32 software, or as a component of an HPLC or LC/MS system controlled by MassLynx" software.

•            As a stand-alone HPLC system controller, the 2790 managen a variety of sample plates while controlling one or morc detectors. Optionally, the 2790 can also control a 3-column selection, 6-column selection, or column regeneration valve.

•            As an HPLC system controlled by Millennium32 software (version 3.2 or higher), the 2790performs sample and solvent management, column selection, and system equilibration.

•            As a component of an LC/MS system controlled by MassLynx (version 3.3 or higher), the 2790 performs sample and solvent management, column selection, and system equilibration.

An LC/MS system that includes the 2790, the Waters ZMD mass spectrometer, and MassLynx software is designated a Waters Alliance® HT LC/MS System (Figure 1-2).

 

System Configurations

The 2790 Separations Module supports IEEE-488 and I/0 connections within a variety of HPLC and LC/MS system configurations.

The 2790 Separations Module can be configured in a stand-alone mode to provide control of up to three UV or RI detector channels as follows:

•            Up to two UV detector channels (a Waters 2487 Dual Detector, single or dual-channel, and/or a Waters 486 Tunable Absorbance Detector)

•            One RI detector channel (Waters 2410 or 410 Differential Refractometer).

The 2790 Separations Module can be configured under Millennium32 software. You use a Millennium32 Chromatography Manager workstation to create methods, which control the Separations Module and other HPLC system components. All detectors that are supported by Millennium32 software can be used wich the 2790 Separations Module. Data from the detectors are sent over the IEEE-488 Interface bus to the Millennium32 software for processing.

In an Alliance HT LC/MS system controlled by MassLynx software, MassLynx can control up to two of the following (one of each):

•            Waters ZMD detector

•            Waters 2487 detector

•            Waters 996 detector

•            Micromassa single- or triple-quadrupole or time-of-flight mass spectrometer

•            Waters SAT/IN" Module

 

Parameter Control

In a stand-alone HPLC System, the 2790 Separations Module can control:

•            Method programming

•            Solvent composition

•            Flow rate

•            Plunger seal-wash flow

•            Sample injection

•            External events

•            Advanced sample management functions including:

–           Rapid equilibration

–           Parallel sample processing

–           Sample pooling

•            Operation of detectors over the IEEE-488 Interface bus

•            Inline degassing

•            Column heating (optional)

•            Sample heating/cooling (optional)

•            Column selection valve (optional)

•            Bar-code reading of sample plates (optional)

With the 2790 Separations Module, you can make parameters such as pressure limits or syringe

draw rates pari of a Separation method. You can program the values of these parameters to change from method to method without having to Set up the Instrument before each run.

 

Spill Protection

All fluid-handling areas of the 2790 haue spill protection; spilled solvent is routed to waste line connectors below the front panel. A drip tray is provided for the top cover if you place a detector an top of the 2790. A solvent bottle tray provides storage for up to four 1 -L solvent reservoirs.

 

Methods Storage and Retrieval

You can Store up to 60 methods (methods include separation methods and sample sets) in the 2790. When the number of stored methods approaches the maximum (60), the delay when you create and saue methods increases to more than 30 seconds. When 60 methods haue been stored, a warning message appears indicating that storage capacity has been reached.

The 2790 can export and import separation methods and sample sets from Standard PC-formatted, 3.5-inch floppy disks using the built-in floppy disk drive.

The 2790 also Supports import of sample sets created and exported using a PC-based Spreadsheet application or text editor in ASCII Format.

 

Record-Keeping Functions

The 2790 automatically records:

•            Total number of injections

•            Total solvent usage (pumped through the System)

•            System errors

•            Programmed operating conditions for each run

•            Column selection This information can be:

•            Printed using a connected serial printer

•            Transferred to an external device, such as the Waters 746 Data Module

•            Exported to a 3.5-inch floppy disk as an ASCII Eile

 

Sample Heater/Cooler

The 2790 can be shipped with the optional sample heater/cooler that maintains the sample compartment at temperatures from 4 to 40 °C. The sample heater/cooler is factory-installed on the 2790XE.

 

Column Heater

The 2790 Column Heater maintains the column at temperatures from 5 °C above ambient (minimum of 20 °C) to 60 °C. You can enable an alarm to warn you if the temperature varies outside the range you specify. The procedure to install the column heater is described in Section 2.3, Installing the Column Heater. The 2790XE includes the column heater.

The 2790 Column Heater is shipped with either no valve or with one of three optional column-selection valves and the associated tubing and connectors. See Section 1.4, Options and Accessories, for information on the column selection valves used with the 2790.

For more information on column heater options, sec Section B.3, 2790 Module Options.

 

Specifications

Height

22.5 in. (57 cm)

Depth

23.5 in. (60 cm)

Width

23 in. (58 cm)

Weight

136 lb. (62 kg)

Wetted Surfase Materials

316 stainless steel, UHMWPE, sapphire, ruby,

Tefzel® (ETFE), Teflon® (FEP and PTFE), PEEK,

Fluoroloy G, Fluoroloy-08R

Operating Temperature

4 to 40 °C

Relative Humidity

20 to 80%, noncondensing

Acoustic Noise

<65 dB(A)

Solvent Compatibility (see Appendix D,Solvent Considerations)

Solvents consistent with materials of construction.

Salts and buffers can reduce seal life, especially at

pressures in excess of 3000 psi.

Line Voltage

85 to 264 VAC

Frequency

47 to 63 Hz

Number of Solvents

One to Tour, three with vacuum degas

Solvent Conditioning

Vacuum degas, three Solvents plus purge solvent

Typical Operating Flow Rate Range

0.050 to 5.000 mL/min in 0.001-mL/min

increments

Programmable Flow Rate Range

0.000 and 0.010 to 10.000 mL/min in

0.001-mL/min increments

Compressibility Compensation

Automatic and continuous

System Delay Volume

<400 µL, independent of backpressure, 1 mL/min

Plunger Seal Wash

Integral, active, programmable

Gradient Profiles

Eleven (11) gradient curves [including linear, step

(2 curves), concave (4 curves), and convex (4

curves)]

Dry Prime/Wet Prime

Automatic, front panel control

Flow Ramping

Time (0.01 to 30.00 min in 0.01 -min increments) to

resch maximum flow rate

Maximum Operating Pressure

5000 psi (345 bar) at 0.010 to 3.000 mL/min;

Programmable upper and lower limits

Composition Range

0.0 to 100.0% in 0.1% increments

Composition Accuracy

±0.5% absolute, independent of backpressure

(Proportioning Valve Pair Test [degassed

methanol:methanol/propylparaben, 2 mL/min, 257

nm])

Composition Precision

≤0.15% RSD or ≤0.02 min SD, whichever is

greater , based on retention time. (Degassed 60%

methanol:40% watet Dial-a-Mix, 1 mL/min, six

replicates, phenone mix, 257 nm)

Flow Precision

≤0.075% RSD or 50.02 min SD, whichever is

greater, based on retention time (N = 6) or

volumetrie measures (0.200 to 5.000 mL/min),

isocratic premix

Flow Accuracy

±1% or 10 µL/min, whichever is greater, (0.200 to

5.000 mL/ min), degassed methanol, at 600 psi

backpressure

Number of Sample Plates

Total of four plates:

•            Microtiter plate – 96- or 384-well

•            Vial plate – 2.0-mL vial (48)

•            Tube plate – 0.5-mL microcentrifuge tube

(48) or 1.5-mL microcentrifuge tube (24)

•            Open access plate – 2.0-mL vial (24 or 48)

Sample Temperature Control

4 to 40 °C, programmable in 1 °C increments

Maximum Sample Capacity

1536 in four 384-well plates

Number of Sample Injections

1 to 99 injections per sample

Sample Delivery Precision

<0.3% RSD, full loop 50 µL. (Default wash/purge

conditions, degassed 60% methanol:40% water

Dial-a-Mix, 1 mL/min, six replicates, paraben mix,

257 nm)

Sample Volume Linearity

>0.999% correlation, 5 to 20 µL, partial fill in‑

50-µL loop, 3-µL pre- and post-sample air gaps

(Default wash/purge conditions, degassed 60%

methanol:40% water Dial-a-Mix, 1 mL/min,

six replicates, paraben mix, 257 nm)

Needle Wash Solvents

Two: wash (strong solvent) and purge (sample‑

compatible) solvent

Sample Carryover

<0.01 % or <2.5 nL (default wash/purge volumes),

whichever is greater. (Blank injection, 25 µL, 60%

methanol:40% water, alter six replicates, 25 µL

propylparaben, 1 g/L, 257 nm)

Parallel Sample Processing

User-programmable next-sample aspiration and

loop fill, column equilibration, just-in-time

gradicnt delivery

Advanced Operations

Auto addition, sample pooling, open access,

priority samples

Column Heater

20 °C (5 °C above ambient) to 60 °C, in 1 °C

increments

Column Selection

3- or 6-column select valve (optional)

IEEE-488 Interface

Control of Waters IEEE-488 equipped detectors;

communication wich Millennium32

Chromatography Manager workstations or

MicroMass detectors using MassLynx software

RS-232 Interface

Output of ASCII text files to a printer/PC/integrator

(Port A)

Floppy Disk Drive

1.44-MB, 3.5-inch floppy dick, for methods

transfer and archiving; reportable GLP log; sample

list Import from ASCII file

Event Inputs

Three TTL or switch closures

Programmable Event Outputs

Six contact closures

 

 

 


2700 Sample Manager

The Waters 8 2700 Sample Manager is a high-capacity sample processing system for the management of sample injection in high-performance liquid chromatography (HPLC), liquid chromatography–mass spectrometry (LC–MS), or flow injection into a mass spectrometer. The 2700 Sample Manager automates sample aspiration and injection from microtiter plates, test tubes, Eppendorf tubes, or conventional autosampler vials. When the available options are installed, the instrument can provide single-point management of sample pretreatment, column selection, injection, and collection of separated fractions. Figure 1-1 shows the major parts of the instrument.

 

 

The 2700 Sample Manager can function as a component of a single Millennium 8 Software-based HPLC system or as part of one system in a multisystem Millennium chromatography Manager configuration.

 

The 2700 Sample Manager is controlled by software installed an a computer that is running Windows— 3. 1, Windows 95 -, or Windows NT". The control software may be operated independently or with a DDE link to Waters Millennium Chromatography Manager (version 2.15.n) that is running Windows 3.1. The 2700 Sample Manager connects to the computer through an RS-232 post and triggers Operation of an HPLC module by transistor-to-transistor logic (TTL).

 

Specifications

Footprint (width x depth x

height)

22 in. x 18 in. x 19 in. (55.9 cm x 45.7 cm x 48.3 cm)

 

Workspace

15.1 in. x 5.9 in. x 6.9 in. (38.4 cm x 15.0 cm x 17.5 cm)

 

Ventilation

At least 1 in. (2.5 cm) from a wall or obstructing surface

 

Weight

Approximately 65 pounds (30 kg)

 

Safety

UL, C-UL, CE, IEC 1010-1

 

Operating temperature

15 °C to 40 °C (59 °F to 104 °F)

 

Operating environment

Indoor use

 

Relative humidity

Maximum relative humidity 85% for temperatures up to

31 °C, decreasing linearly to 50% relative humidity at 40 °C

 

Storage temperature

0 °C to 50 °C (32 °F to 122 °F)

 

Pollution

Degree 2

 

Altitude

Up to 2,000 M (6562 feet)

 

Power supply input

110/230 Vac (10% at frequencies from 47 Hz to 63 Hz).

Input selection is fully automatic. Requires earth-grounded

power source.

 

Fuses

Two 3.15-A fuses at the input module.

 

Power supply Output

Genrates 24 V. All devices internal to the Instrument

operate an 24 V.

 

Installation category

Overvoltage Category II.

 

Input voltages

Auto-selecting 110/230 Vac (10%).

 

Frequency

47 to 63 Hz.

 

Maximum power

150 watts.

 

Item

X-Axis Specification

Y-Axis Specification

Z-Axis Specification

Travel range

383 mm (15.08 in.)

150 mm (5.91 in.)

165 mm (6.50 in.)

Travel range

(steps)

1750 steps

1065 steps

1782 steps

Initialization

Offset

5 steps

5 steps

40 steps

Resolution per

half step

0.2234 mm (0.009 in.)

0.1422 mm (0.006 in.)

0.0982 mm (0.004 in.)

Accuracy over

travel*

+0.20 mm (±0.008 in.)

±0.20 mm (±0.008 in.)

±0.40 mm (±0.016 in.)

Reproducibility*

±0.10 mm 0-0.004 in.)

±0.10 mm (±0.004 in.)

±0.10 mm (±0.004 in.)

Start speed

50 steps/sec

11 mm/sec

(0.43 in./sec)

200 steps/sec

28 mm/sec

(1.1 in./sec)

400 steps/sec

39 mm/sec

(1.54 in./sec)

End speed

4,000 steps/sec

894 mm/sec

(35.2 in./sec)

4,000 steps/sec

569 mm/sec

(22.4 in./sec)

4,000 steps/sec

393 mm/sec

(15.5 in./sec)

Acceleration

10,000 steps/sec'

2,235 mm/sec2

(87.9 in./sec')

20,000 steps/sec'

2

2,845 mm/sec'

(112 in./sec')

30,000 steps/sec'

mm/sec'

(116.0 in./sec')

Item

Description

Injector volume (fixed loop)

20 µl- Standard; 5µL, 10 µL, 50 µL, 100 µL, 250 µL,

500 µL, 1.0 mL, 2.0 mL, and 5.0 mL available.

Syringe sizes

100 µL, 250 µL, 500 µL, 1.0 mL, 5.0 mL.

Resolution

Mechanical resolution is 1/3,000 of syringe volume.

Smallest recommended volume is 24 steps or 2µL,

whichever is the larger volume.

Injection accuracy

> 99% at füll stroke wich 500-µL syringe

Precision

< 0.75% RSD; 20-µL injection volume, 20-µL fixed loop,

overfill mode, six replicates; phenone mix, 254 nm; eluent

and Sample diluent: degassed methanol:water, 60:40,

premixed; Symmetry® C 18 column, 3.9 x 50 mm; 1 mL/min

Carryover

< 0.1%

Injector cycle time

< 20 sec

Computer operating System

Windows 3.1, Windows 95 or Windows NT Mrunning on an IBM PC or compatible.

Communication

RS-232 serial interface

Floppy diskette drive

3.5 Inch, 1.44 MB

 

 

 


PDA-Detektor 996

 

 

Specifications

Dimensions

11.5 x 22 Inches (29 x 56 cm)

Weight

31 lbs (14.3 kg)

Wavelength range

190 to 800 nm

Wavelength accuracy

±1 nm

Linearity range*

5% at 2.0 AU, propylparaben,

at 258 nm

Spectral resolution

1.2 nm

Baseline noise

±1.5 x 10-5 AU peak-to-peak, dry,

at 254 nm

Drift

1 x 10-3 AU/hour

at 254 nm (after warmup)

AT:9 1°C per hour

Flow cells

Standard

Semi-preparative

Microbore

Inert

Pathlength (mm):        Tubing (I.D.)

10         0.009 in

3           0.040 in

3           0.005 in

10         0.010 in

 

 

 


PL-ELS 1000

 

Introduction

The PL-ELS 1000 evaporative light scattering detector or mass detector is a unique and highly sensitive detector for non-volatile solutes in a volatile liquid stream. lt is mainly used as a concentration detector in Gel Permeation Chromatography (GPC) and other forms of Liquid Chromatography. The solvent stream containing the solute material is nebulized and carried by a gas flow through an evaporating chamber. The solvent is volatilised, leaving a miss of solute particles that scatter light to a photosensitive device. The Signal is amplified and a voltage output results. The output is directly related to the "mass" of the solute particles passing through the light, hence the narre "Mass Detector".

The PL-ELS 1000 may be used alone, or as one of several detectors in a GPC or Liquid Chromatography System. As the solvent or eluent is evaporated in the course of the analysis, the PL-ELS 1000 must be the last in series if used in conjunction wich other detectors. If the PL­ELS 1000 is being used as the last detector in a series, care must be taken not to exceed the recommended back-pressure in detector cells in other units.

 

Specifications

Light Source                                                               Tungsten/Halogen Lamp

Detector                                                                     Photodiode

Temperature Range *     Evaporator                           30-300°C

                                      Nebulizer                              30-220°C

                                      Heated Transfer Line           30-220°C

Gas Flow                                                                    0-2 SLM @60 PSI@25°C

                                      Pressure operating range    60 – 100 PSI (4-6.7 Bar)

                                      Maximum Pressure             150 PSI (10 Bar)

Eluent Flow                                                                0-5ml/min

Analogue Output                                                        O-10V

                                                                                  O-1V

Communication                                                         Serial I/0

                                      Outputs                                2 Contact closures

                                                                                  1 TTL +ve

                                                                                  1 TTL –ve

                                                                                  Heated Transfer live control

                                      Input                                     Remote auto-zero control

Instrument Control                                                     Microprocessor

Instrument Interface                                                   Detachable IR remote control

                                                                                  Windows based PC control

Detector Status                                                          Sleep, Gas Save, Standby, Hearing, Ready

                                                                                  and Error

Size                                wxdxh                                   175x480x430mm

                                      Packaged wxdxh                  670x340x580mm

Weight                                                                        15Kg

                                      Packaged                             22Kg

Product groep: HPLC

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