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Finnigan TSQ API1 7000

Seriennummer: 013732
Stato: Archived Product?The unit is no longer available.
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Objektnummer B00013732
Seriennummer 013732
Nome oggetto Finnigan TSQ API1 7000
Stato Archiv

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The second-hand devices are verified by Labexchange Service GmbH before delivery. You are receiving only fully functional devices.

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The stated dispatch times are the shortest possible ones for each article. The effective dispatch times can vary. The effective dispatch times will be stated in the order confirmation.

As a matter of principle, we are offering collective deliveries. The shipping time is calculated based on the position with the longest lead time. A partial delivery is possible on explicit request.

 

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The stated transport and packing charges apply to the most favorable route if transport and are to be understood as subject to verification due to unexpected cost increases. By reason of unpredictable events, cargo rates and delivery times can change at any time and therefore have to be adapted to the recent situation. Import formalities and possible customs charges will be borne by the purchaser. Incoterm coding according to Incoterms 2010: For persons who collect the devices themselves: EXW, for dipatch by sea: CFR, by air freight: CPT, other shipments: DAP. Note for international shipments: A proof of preference/EUR1 will not be issued by us. When self-collecting/ordering EXW from countries within or outside the European Union, 16% VAT will be retained as a deposit until we have received the corresponding confirmation of arrival/bill of delivery from the buyer.

 

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We do not accept payment by letter of credit, PayPal, etc. In each case the invoice amount is payable without deduction. Discount is not granted.

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DE, AT, CH

Payment by invoice, payment in advance, payment by credit card

Payment by invoice is only possible for corporate clients.

NL, BE, LU

Payment by invoice, payment in advance, payment by credit card

Payment by invoice is only possible for corporate clients

Other countries

Payment in advance, payment by credit card

 

 

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The goods are offered subject to prior sale.

 

Definition of status

All articles are used articles, except an article is listed especially as a new device.

Status

Condition

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Immediately available

Used The article is fully functional and in impeccable condition. It can be shipped immediately.
In stock

Used

The article is on stock. Our service technicians will verify the article before delivery. You are receiving only a fully functional article.

Published

Used

The article is still with the provider. After your order the article will be purchased and verified by us before being shipped to you. A certificate of operativeness as well as a service report are included in delivery.

New device

new

The article is brand new and unused. Regarding new equipment the guarantee/warranty conditions of the corresponding manufacturer apply.

Labprocure

Used

Labprocure GmbH, as the advertiser, is responsible for the content of this device offer. Labprocure assumes liability for the offers advertised here and for the photos and offer texts included. Labprocure GmbH, Bruckstraße 58, 72393 Burladingen.

Firma:              Finnigan

Modell:            TSQ API1 7000

Kommentar:   Dokumente engl.

The following illustrations and descriptions are referring to the instrument model and are drawn from brochures. They are not representing the delivery volume. The exact delivery content you will find only in the offering text.

TSQ® 7000

Triple-Stage Quadrupole Mass Spectrometer

The TSQ 7000 is the next generation in triple-stage quadrupole technology, the most advanced, versatile, and powerful mass spec­trometer available in its class.

The 7000 Series features new, longer quad­rupoles for improved resolution, a non-linear octapole collision cell providing efficient collision-induced dissociation (CID) and neutral noise reduction, an advanced 15 kV conversion dynode detector to enhance sensitivity, and digital signal processing for improved detec­tion limits.

The TSQ also offers the most complete range of sample introduction techniques available for unequaled versatility. Advanced MS/MS capabilities enable you to solve virtually any analytical problem today, and into the future.

Standard Features

Mass Spectrometer

Mass Analyzer

•            High precision 250 mm hyperbolic quadrupole mass analyzers with dual 2500/4000 u mass range, switchable from the data system terminal

•            MS and MS/MS analysis an alternate scans

•            Mass peak position stable to 0.05 u over 8 hours (alter warmup)

Collision Gell

•            Non-linear octapole assembly with 185 mm collision path length for efficient ion fragmentation and neutral noise reduction

•            Ion collision energies of 0 to ±196 eV, program­mable scan-to-scan

•            Innovative cell enclosure provides operating pressures from 0.1 to 10 mTorr (13-1300 mPa)

Detector

•            Post-acceleration conversion dynode with -15 kV or +15 kV applied voltage for detection of positive or negative ions, respectively

•            Off-axis continuous dynode electron multiplier with extended dynamic range, operable to -3000 V

•            Unique direct mounting of the multiplier to the electrometer PCB to eliminate microphonic­induced anode noise

Vacuum System

•            Cradle vacuum system with glass plates sealing the ion source and mass analyzer chambers

•            Hybrid turbomolecular/molecular drag pumps

•            Three inlet ports to simultaneously support GC, Particle Beam, and probe interfaces in EI/CI modes

Acquisition Interface

•            Automatic bandwidth optimization of the analog­to-digital converter (ADC) up to 45 kHz maximum

•            Up to 50,000 digital samples per scan, or 100,000 samples per second, can be acquired at scan rates as high as 4000 u s-'.

•            Programmable digital signal processor (DSP) with 48-bit precision for all data acquisition calculations (including centroiding, averaging, profile data accumulation, background subtraction, and real-time deconvolution) and electronic noise discrimination

•            DSP's 48-bit internal dynamic range yields external dynamic range of 2.6 x 108 for centroid data and 2.38 x 108 for profile data

•            Five analog inputs, two analog outputs, four RS-232 serial interfaces, and three TTL input/output lines for interfacing to other instruments

Data System

Hardware

•            High-performance 64-bit Alpha AXP" RISC-based workstation, with OSF/1® operating system

•            Storage expansion module with high-capacity disk drive, CD-ROM and DAT tape drive

•            High resolution monitor

•            PostScript® laser printer

•            Ethernet" port for connection to mass spectrom­eter and laboratory networks

Software

•            Instrument Control Language'" with GUIDE" step‑by-step control and ICIS"11 applications software—mouse driven or keyboard control, multi-window‑ing environment with Motir graphical user interface

•            TCP/1P networking software for connecting to any remote workstation, including PCs, Macintosh®computers, and X-terminals

Instrument Control

•            All ion path parameters can be programmed with the mass scan. Independent parameter sets can be stored for different Operation modes (e.g., ESI, APCI, El, Cl, positive/negative ion, different collision energies, etc.).

•            Data system control of all major GC, LC, and GC/ LC autosamplers, such as Varian 3400, A200S, HP 5890, Waters 6000/717, HP 1050, TSP 4100, and Michrom. Control includes:

–           setting operating parameters

–           setting up, saving, and downloading methods

–           reading status

– controlling an automated analysis

•            Comprehensive diagnostic programs for real-time analysis of system performance

Performance Specifications

LC/MS Sensitivity

Atmospheric Pressure Chemical Ionization (APCI):

•            A loop injection of 5µL of a 10 pg µL -1 solution of reserpine [50 picograms (82 femtomoles) total sample] at 1 mL min -1 of 50% methanol/50% water with 1% acetic acid will produce a minimum peak-to-peak signal-to-noise ratio of 10:1 for the protonated molecular ion at m/z 609 when the mass spectrometer is operated in a selected-ion­monitoring mode scanning a 1 dalton wide window at m/z 609 in 0.2 s.

Electrospray (ESI):

•            A loop injection of 1µL of a 50 pg 1.1L -1 solution of reserpine [50 picograms (82 femtomoles) total sample] at 200 µL min -1 flow of 50% methanol/ 50% water with 1% acetic acid will produce a minimum peak-to-peak signal-to-noise ratio of 10:1 for the protonated molecular ion at m/z 609 when the mass spectrometer is operated in a selected-ion-monitoring mode scanning a 1 dalton wide window at m/z 609 in 0.2 s.

Thermospray (TSP TM ):

•            With a mobile phase of 20% methanol/80% water with 0.05 M ammonium acetate buffer at a 1.2-1.5 mL min -1 flow rate, the Signal produced by injection of 20 µL of a solution of 0.5 ng µL -1 of adenosine into a 20 µL injection loop will yield a minimum peak-to-peak signal-to-noise ratio of 50:1 for the protonated molecular ion at m/z 268 when the mass analyzer is scanned in an MS mode from m/z 120 to 280 in 0.5 s.

Particle Beam Interface (PBI):

•            With an ion source temperature of 250 °C, desolvation chamber temperature of 40 °C, helium gas for nebulization at a pressure of 40 psi, and mobile phase of 100% methanol at a 0.3 mL min -1 flow rate, the following specifications will be met:

El: Upon injection of 5 µL of a solution of 2 ng µL -1 of caffeine in methanol, the system will produce a minimum peak-to-peak signal-to-noise ratio of 10:1 for the molecular ion at m/z 194 when the mass analyzer is scanned in an MS mode from m/z 65 to 250 in 1 s.

Cl: Upon injection of 5µL of a solution of 2 ng 1.tL-1 of caffeine in methanol, the system will produce a minimum peak-to-peak signal-to-noise ratio of 10:1 for the protonated molecular ion at m/z 195 when the mass analyzer is scanned in an MS mode from m/z 65 to 250 in 1 s.

GC/MS Sensitivity

Electron Ionization (EI):

•            Upon a splitless injection of 200 pg of methyl stearate onto the fused silica capillary column provided with the system, the system will produce a minimum peak-to-peak signal-to-noise ratio of 30:1 for the molecular ion at m/z 298 when Q1 is scanned from m/z 60 to 310 in 0.5 s.

Chemical Ionization (CI):

•            Upon a splitless injection of 100 pg of benzo­phenone onto the fused silica capillary column provided with the system, the system will produce a minimum peak-to-peak signal-to-noise ratio of 25:1 for the protonated molecular ion at m/z 183 when Q1 is scanned from m/z 90 to 240 in 0.5 s using methane as the reagent gas.

MS/MS Efficiency

Collision-Induced Dissociation (CID):

•            Upon a splitless injection of 100 pg benzo­phenone onto the fused silica capillary column provided with the system, the system will produce a minimum peak-to-peak signal-to-noise ratio of 50:1 for the m/z 105 product ion of m/z 183 when the system is operated in the product ion mode and Q3 is scanned from m/z 50 to m/z 185 in 0.5 s using methane as the reagent gas, a colli­sion energy of -20 eV, and a collision gas pres­sure of 1 to 2 mTorr (130-260 mPa).

Optional Features

The versatility and flexibility of the TSQ 7000 are unmatched. A range of options is available, including:

EUCI Ion Source

•            High performance ion source for El, positive ion Cl, and negative ion Cl Operation

•            Patented exchangeable ion volumes allow rapid switchover between EI and Cl

•            Up to 2 mA emission current and electron energies of-l0 to-190V

LC Interfaces

•            Atmospheric Pressure lonization (API) including Electrospray (ESI) and Atmospheric Pressure Chemical lonization (APCI) inlets, providing source fragmentation in either the capillary/skimmer region or source octapole, under complete data system control

•            Particle Beam Interface

•            TSP2 TM with filament and discharge ionization capability

•            Supercritical fluid chromatography (SFC)

Gas Chromatograph

•            High-performance capillary GC with multi-linear programming and split/splitless capillary injector

•            Independently heated, direct coupling capillary interface, operable to 400 °C

•            On-column injector

•            Autosampler

Probes

•            Liquid-cooled solids probe with ion current feedback control

•            Desorption chemical ionization (DCI) probe

•            Fast Atom Bombardment (FAB)

•            BioProbe TM (continuous flow FAB)

Data System

•            NIST (NBS) mass spectral library

•            Wiley mass spectral library

•            High-speed/high-output laser printer

•            Additional workstation memory

•            Optical disk drive

•            PC workstation

Installation Requirements

Power

Power: Two 220 V ac -5%+10%, 50/60 Hz at 30 A.

Stable voltage, free of spikes, sags, and surges.

Please refer to the Preinstallation Guide for complete specifications.

Environment

System averages 3500 W (12,000 Btu h -1 ). Ambient environment must be 15-26 °C (59-80 °F) with a relative humidity of 20-80% with no condensation.

Dimensions/Weight

Mass spectrometer: 151 cm h x 60 cm w

(allow extra 55 cm [24 in] for card cage removal)

x 118 cm d (60 in x 24 in x 46 in).

Weight: 360 kg (790 Ib).

GC cabinet: 86 cm h x 56 cm w x 59 cm d

(34 in x 22 in x 23 in), provided with GC Option

Data system table: 66 cm h (1340 cm h [53 in] with computer and terminal) x 121 wx 81 cm d. (26 in x 48 in x 32 in).

Gruppo prodotti: LC / MS

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