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Beckman HPLC

Seriennummer: 005633
Status: Archived Product
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Descrizione:
Beckman HPLC sistema. Mit Pumpe 126. Probengeber Oro 507.Detektor 168. Gold-Software. PC. Tenere Sotto Controllo. Zubehör.
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Objektnummer B00005633
Seriennummer 005633
Nome oggetto Beckman HPLC
Stato Archived Product

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All articles are used articles, except an article is listed especially as a new device.

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new

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Labprocure

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Labprocure GmbH, as the advertiser, is responsible for the content of this device offer. Labprocure assumes liability for the offers advertised here and for the photos and offer texts included. Labprocure GmbH, Bruckstraße 58, 72393 Burladingen.

Firma:              Beckman

Modell:            HPLC

Kommentar:   Dokumente für IDNR 9744

System Gold HPLC

bestehend aus:

·        Rheodyne Inj.-ventil 9725i

·        DynaLoop

·        Pumpenmodul 126

·        DAD 168

·        BioFrac Fraction Collector

·        Unichromat 1500

·        PC/Workstation V5.00

·        Monitor, Drucker

Ø       Rheodyne Inj.-ventil 9725i

DESCRIPTION

Models 7725(i), 9725(i), 3725(i)-038, 3725(i), and 9125 are six-port sample injection valves in which the sample is loaded through a built-in needle port in the front of the valve. Models 7725(i) and 3725(i)-038 are the stainless steel versions, and Models 9725(i), 3725(i), and 9125 are the PEEK versions.

The 'i" version of each model includes a built-in position sensing switch.

LOADING BY SUCTION

The two preceding methods expose the sample to the metal needle of the loading syringe. Metal can be completely avoided by using a syringe to suck sample into the loop.

The steps are as follows:

a) In LOAD, dip the tube attached to Port 6 into the sample.

b) Insert an empty syringe into the needle port and suck up sample into the loop. Alternatively, use the Suction Needle Adapter (P/N 9125-076, not supplied).

c) Leave the syringe in position and turn to INJECT.

The metal needle of the syringe will contact the sample if an excess of sample is drawn into the syringe, but this excess sample is external to the sample loop and will not be injected. The syringe can be used many times before it needs to be emptied.

To load the loop with all of the available sample, the loop should be at least four times the volume of sample loaded. The loop is first filled with mobile phase via the dip tube, then the whole sample is drawn into the dip tube and loop, followed by more mobile phase. The sample is now sandwiched between two zones of mobile phase in the loop.

Loading by suction using the Suction Needle Adapter.

Ø       DynaLoop

DynaLoop Sample Loop Description

The DynaLoop Sample Loop is a large-volume sample injection loop for use with the BioLogic System. Available in 25 ml and 90 ml sample capacities, the DynaLoop can be used with either the manual V7-3 or automated AV7-3 injection valve.

Operation

The DynaLoop consists of five major components (Figure 1):

•     Sample end assembly

•     Buffer end assembly

•     Glass tube graduated in 1 ml increments

•     Sliding seal assembly

•     Protective plastic jacket

DynaLoop 25 and DynaLoop 90 Sample Loops

Ø       Pumpenmodul 126

Das Pumpenmodul 126 für Gradientenbetrieb fördert 0,001 bis 10 ml/min.

Das Einkolben Design mit elektronischer Echtzeit Kompressibilität-Kompensation gewährleistet konstanten und pulsfreien Fluß, unabhängig von Laufmittel und Druck. Die Hinterkolbenspülung verhindert das Auskristallisieren von Salz.

Im Modul 126 integriert befindet sich der doppelstufige dynamische Mischer für hochdruckseitige Gradientenformung.

Programmierbare Eluentenselektoren ermöglichen die automatische Lösungsmittelauswahl aus 4 Vorlagen pro Pumpe.

Ø       DAD 168

Der Diodenarray-Detektor Modell 168 bietet folgende Spezifikationen:

-       512 Dioden

-       Analytische Standard-Flußzelle:

11 ul Zellvolumen, 10 mm Weglänge

-       Auf Wunsch semi-präparative Flußzelle:

2 mm Weglänge

-       Wellenlängenbereich: 190 - 600 nm

-       Wellenlängengenauigkeit: ± 1 nm

-       Bandbreite: Variabel von 4 nm bis zum gesamten Wellenlängenbereich

-       2 Datenkanäle + 1 Referenzkanal

-       Basislinienrauschen: kleiner 1 x 10 (-4) AU

-       Drift: kleiner 2 x 10 (-3) AU/h

-       Meßbereich: 0.001 bis 1.5 AUFS

-       Variable Rise-Time: 0 - 5 sec

-       Datenrate: 1, 2, 4, 8 oder 16 Hz

-       Autozero

-       Peakerkennung für die Scan-Funktion bzw. zur Steuerung eines Fraktionssammlers

-       Scan-Arten: in frei wählbaren Intervallen, am Peakmaximum, zur Reinheitskontrolle,bei Detektion einer Verunreinigung

-       Scanrate: 0.5 bis 16 Hz

-       Spektrale Bandbreite: kleiner 4 nm

-       Real-Time Scan während der Datenaufnahme

-       Software zur Real-Time Peakreinheitsbe-. stimmung: ein graphisches Symbol unter dem Chromatogramm zeigt die Anzahl der Verunreinigungen an

-       Pro PC kann nur 1 Diode-Array Detektor 168 betrieben werden

-       bestehend aus:

Diode-Array Detektor 168

Scan-Graphik Software


Ø       BioFrac Fraction Collector

Physical Description

                      

Rack

ID

Rack Description

Rack

Capacity

Format

Columns x Rows

Tubes

Per Rack

(Total)

F1

Holds 12-13 mm diameter

tubes up to 150 mm in height

2 racks

6 x 15

90 (180)

Ice bath/ microplate rack

Ice bath for 13 mm diameter tubes. This rack also serves as a holder for 12-, 24-, 48-, and 96-well microplates and microtiter tubes that adhere to the SBS standard format.

1 rack

10 x 12

120

Ø       Unichromat 1500

Das Gerät dient ausschließlich zur Lagerung von Lebensmittelprodukten. Die Produkte sind unter Beachtung der aufgeführten Ladekapazität und unter Gewährleistung der einwandfreien Luftzirkulation im Geräteinnern zu lagern.

Ladekapazität in mm                                      L:530                H: 1200            P: 650

Öffnungsmaße eines Gerät-Kühlfachs:         L: 600               H: 1500

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