Bruker AXS Smart Apex CCD
Objektnummer | B00017509 |
---|---|
Numéro d'identification | 017509 |
Nom de l'objet | Bruker AXS Smart Apex CCD |
Statut | Archiv |
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manufacturer : Bruker
model : AXS Smart Apex CCD
annotation : Dokumente engl.
The following illustrations and descriptions refer to the instrument model and are drawn from brochures. They do not represent the scope of delivery. Please refer to the text of the offer for the exact scope of delivery.
SMART APEX CCD Detector
Construction 4K CCD phosphor mechanically coupled
Imaging Area 62 mm x 62 mm
Demagnification Ratio 1:1 (unit demagnification)
Gain, Mo >170 electrons/X-ray photon
Number of Pixels 4096 x 4096
Front End Pixel Size 15 µm x 15 µm
Selectable Frame Sizes 512 x 512, 1024 x 1024
Number of Ports Readout 4
Selectable Readout Speeds per Port 200 K pixels/s, 370 K pixels/s
Readout Time at 370 K/s 512 x 512 0.2 s
( effective 1.5 MHz readout) 1024 x 1024 0.7 s
Effective Digitization Range 20 bits (25 bits with attenuator)
Crystol-to-Detector Window Distance, d 25 mm - 250 mm
D8 Goniometer, horizontal
Max. Range, Subject to Detectors Max. Speed, Subject to Detectors
Axis or Accessories Mounted or Accessories Mounted Reproducibility
20 360° 1500 degrees/min ±0.0001°
ω 360° 1500 degrees/min ±0.0001°
Ø 360° 2000 degrees/min ±0.0005°
X fixed, 54.74°
Optics 0.3, 0.5, 0.8 mm pinhole collimators, graphite crystal monochromator standard with sealed tube systems
Color Video Camera included with D8 goniometer
MonoCapTM Optic (option) 1000, 500, 300, 100, or 50 µm diameter
X-ray Generator (solid state) Input voltage: 205-240 VAC 30 A , 50/60 Hz single phase
Sealed Tube Output voltage: 10-60 kV
Output current: 2 - 80 mA
Stability, kV and mA ±0.01% at 10% fluctuation
Microprocessor controller with automatic startup and burn-in cycling for X-ray tubes
Ceramic X-ray Tubes Mo, normal focus 2400 watt or fine focus 2000 watt
Cu, normal focus 2000 watt or fine focus 1500 watt
Host Computer PentiumTm-based PC with local mass storage, color SVGA display, and network communications
and Software SMART, VIDEO, RLATT, GEMINI, SADABS, ASTRO/COSMO, SAINT+, FINDSYM, SHELXTL,
XSHELL included. GADDS optional.
KRISTALLOFLEX© 760 X-ray Generator
Powerful for all X-ray diffraction tubes and other side-window tubes:
100/80 mA current or 60 kV voltage with 3 kW output power
Easy Operation with
automatic control via microprocessor and external PC or manual control
FLEX-CONTROL, the program for PC control of the generator as stand-alone device (e.g. with film camera measuring stations)
efficient diagnostic information
Protecting X-ray tubes with
automatic start-up routine
immediate switch-off at tube flashovers (guarantees spectral purity)
controlled automatic increasing up to operational values after tube flashovers
automatic standby mode
Universal application:
window control for four tube windows (option)
compact design for installation in standard 19" racks
use in diffractometers, film camera measuring stations, spectrometers with side-window tubes and rotating anodes
Ecological and economical because of
water switch-off in stand-by mode (option)
minimized current consumption (patented circuitry)
considerable saving of water using facility for connection to the internal cooling-water unit
Technical data KRISTALLOFLEX 760-80 KRISTALLOFLEX 760-100
Continuous output power Max. 3 kW
High voltage 10 to 60 kV
Tube current 2 to 80 mA 2 to 100 mA
Frequency 20 kHz
Stability of high-voltage and tube current with ≤ 0.01
mains fluctuations up to ± 10 %
High voltage ripple ≤ 5 %
Regulation time constant < 100 ms
Tube heating current 2 to 4.5 A
Tube heating voltage 5 to 12 V
Power supply 230 V ± 10%, 50/60 Hz
Power consumption 5.5 kVA
Mains fuse 25 A , slow-blow
Cooling-water connection 1/2"
Cooling-water flow rate Min. 3.5 1/min 1)
Water pressure 5 to 8 bar 2)
Water temperature 10 to 35 °C
Degree of protection to DIN 40050 IP 20
Dimensions (w x h x d)
Desk-top version 446 mm x 266 mm x 704 mm
Rack-mounted version 465 mm x 222 mm x 704 mm
Weight
Desk-top version 76 kg
Rack-mounted version 65 kg
1)Reduced minimum values an request.
2)Min . 3 bar with internal cooling-water unit.
KRYO-FLEX LOW TEMPERATURE ATTACHMENT
The KRYO-FLEX Low Temperature Attachment permits crystallographic studies at controlled temperatures by enveloping a crystal sample in low temperature nitrogen gas. The low temperature attachment addresses the need to handle delicate samples and to obtain more accurate structures from small molecules and biological macromolecules.
The KRYO-FIEX features highly stable temperature control with greatly reduced liquid nitrogen consumption. It can be run at low temperature uninterrupted for weeks because of the automafic refill of the local 60 liter Dewar. Ice formation is avoided at the sample by shielding the cold gas stream with gas at ambient temperature.
The KRYO-FIEX features a long 3000 mm flexible insulated stainless steel transfer line allowing it to be mounted easily on different instruments having sealed tube or rotating anode generator enclosures and in synchrotron hutches.
A digital temperature controller and GUI software interface makes it easy to set or change the sample temperature.
KRYO-FLEX Cooler
Liquid Nitrogen Consumption < 0.5 liter/hour due to heat exchange principle
Temperature Stability ± 0.1 degree K at 100K
N 2 Gas Flow Rate User-selected electronically controlled gas flow rate 2.5 to 7.5 l/min
Mount Two position mount for easy sample transfer an and off the goniometer (provided for D8 goniometer or stand-alone installations)
Transfer Line Flexible insulated stainless steel 3000 mm
Pneumatic Unit Unit includes membrane pump for nitrogen gas flow delivery, a dryer cartridge and manual needle valve for dry gas flow rate adjustment Enclosure size 19" rack (installed in D8 enclosure)
Dry Gas Supply Requirements Air dryer optionally available; dry gas supplied by user must meet requirements:
Dew point < -60° C
10 liters/minute (typical 3-5 liters/minute)
2 bar minimum inlet pressure at pneumatic unit
Temperature Control Unit
Control Electronics Standard 19" rack mount, (installed in D8 enclosure)
Safety Features Check for nitrogen gas flow present
Dewar low nitrogen level detection
Automatic refill
Control Software control directly from Bruker data-collection software or stand‑alone GUI interface
KRYO-FLEX is available as 220V/50Hz or 115V/60Hz version
Air Dryer (optional) Zander KM-5, mounts in D8 enclosure
Bruker AXS ceramic tubes are 100% compatible with the traditional glass tubes for X-ray diffraction.The main benefit of ceramic insulation versus glass insulation is the higher reproducibility of the focal spot position. This facilitates the change of tubes in case of tube replacement or change of wavelength.The improved design of the cathode leads to a longer life compared to conventional glass tubes.The design of the ceramic tubes guarantees state-of-the-art spectral purity.There are two and four window versions available. The standard version is the two window version. lt provides one line and one spot focus and works with the one window tube housings (type S and type P). The four window version is required for three and four window tube housings in double goniometers, goniometers with film camera, and X-ray work benches.A wide variety of anode materials and focus dimensions are available.When disposing of your used tubes: there is a refund toward the purchase of a new tube from Bruker AXS if a used ceramic tube is returned. Like all Bruker AXS products, the ceramic tubes are manufactured according to ISO 9001standards.
Selection of Anode Material with respect to the Application
Anode Characteristic Application
Material a 1 -Radiation (nm)
Characteristic radiation, e.g. Laue exposures on single crystals
Ag Lα 1 0.0559408 When low absorption is desired, e.g. with single crystal
experiments and transmission measurements. The most important reflections occur at relatively small 20 angles, where the Lorentz polarization factor leads to higher intensities. The angular resolution is low. Often used for examinations of steels and metal alloys.
Mo Kα 1 0.070930 When low absorption is desired, e.g. with single crystal
experiments and transmission measurements. The most important reflections occur at relatively small 20 angles, where the Lorentz polarization factor leads to higher intensities. The angular resolution is low.
Cu Kα 1 0.1540562 Ideal for most powder diffraction examinations and thin film
analysis such as high resolution XRD and reflectometry, as
well as light atom single crystal experiments.
Co Kα 1 0.1788965 Used for investigation of ferrous samples where the Fe
fluorescence would cause a high background.
Fe Kα 1 0.1936042 Used for investigation of ferrous samples where the Fe
fluorescence would cause a high background.
Cr Kα 1 0.228970 Provides clear diffraction patterns with well separated
reflections . Ideal for materials with large unit cell dimensions like clay minerals, for complex organic substances, and for stress analysis.
Ti Kα 1 0.2748510 Used for stress analysis.
Technical Data
Maximum voltage 60 kV
Total series resistance 50 kΩ
Max. heating voltage 11 V
Max. heating current 3.8 A
Foreign lines on delivery < 1 %
Increase of foreign lines per 1000h < 0.9%
Cooling water flow-rate ≥ 3.5 l/min
Cooling water temperature ≤ 35 °C
Water pressure ≥ 8 bar
Weight ca. 1.9 kg